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One Step Synthesis and Growth Mechanism of Carbon Nanotubes

查看全文 作  者:Akshay [1,2]Kumar;[2]K.Singh;[2]O.P.Pandey 高影响力作者 机构地区:[1]Sri Guru Granth Sahib World University;[2]School of Physics and Materials Science,Thapar University高影响力机构 出  处:《Journal of Materials Science & Technology》索引2014年第30卷第2期,共5页高影响力期刊 基  金:Council of Scientific and Industrial Research(CSIR)India,for providing financial assistance 摘  要:A simple one step,reproducible,synthesis route for carbon nanotubes was proposed.No external catalyst was used for the synthesis.These nanotubes were obtained after decomposition of acetone at 650 ℃ in a specially designed autoclave.The pressure generated due to decomposition of acetone played a vital role in the synthesis.The X-ray diffraction pattern and transmission electron microscopy of the sample showed that the diameter of nanotubes is in the range of 3—14 nm.The thermo gravimetric analysis showed 3%weight loss below500 ℃;the content of amorphous carbon is very less.The growth mechanism of CNTs was also proposed in the present paper. 关 键 词:一步法合成 碳纳米管 生长机理 透射电子显微镜 合成路线 衍射图案 热重分析 重量损失
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