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Synthesis of the Complex Fluoride LiBaF_(3) through a Solvothermal Process

查看全文 作  者:Rui Nian HUA1, Zhi Hong JIA2, De Min XIE1, Chun Shan SHI2* 1Faculty of Chemistry, Northeast Normal University, Changchun 130024 2Key Laboratory of Rare Earth Chemistry and Physics, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Ch 高影响力作者 出  处:《Chinese Chemical Letters》索引2002年第13卷第10期,共4页高影响力期刊 基  金:This work was supported by the State Key Project of Foundation Research (G1998061306) ;theNational Natural Science Foundation of China (50072031). 摘  要:The complex fluoride LiBaF3 is solvothermally synthesized at 180℃ and characterized by means of X-ray powder diffraction, scanning electron microscopy, thermogravimetric analysis and infrared spectroscopy. In the solvothermal process, the solvents, mole ratios of initial mixtures and reaction temperature play important roles in the growth of the single crystal. 关 键 词:SOLVOTHERMAL synthesis, COMPLEX fluoride.
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